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Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials
Fang Kun,Li Shouping,Cui Longlan,Mao Weimin,Wu Qiye*
Author NameAffiliationE-mail
Fang Kun Department Polymer Science Engineering, Qingdao University of Science and Technology, Qingdao 266042; Department Material Science Engineering, Beijing University of Science and Technology, Beijing 100083  
Li Shouping Department Polymer Science Engineering, Qingdao University of Science and Technology, Qingdao 266042  
Cui Longlan Department Polymer Science Engineering, Qingdao University of Science and Technology, Qingdao 266042  
Mao Weimin Department Material Science Engineering, Beijing University of Science and Technology, Beijing 100083  
Wu Qiye* Department Polymer Science Engineering, Qingdao University of Science and Technology, Qingdao 266042 qiyewu@163.com 
Abstract:
The ultrafine nickel particles/polyaniline nanocomposite materials were synthesized in situ polymerization by two step seriesW/O inverse microemulsion systems. As the first step, the ultrafine nickel nanoparticles whose diameter is 10~30 nm were prepared by the W/O inverse microemulsion systems and by the reduction. As the second step, the monomer aniline salt (AnH+Cl-) entered into the polar water pools where contained nickel nanoparticles and the ultrafine nickel particles/Polyaniline nanocomposite materials whose diameter is 50~100 nm had been obtained by in situ polymerization. These nanocomposite materials were measured to characterize and the micromorphology, microstructure and physical interaction of the both ultrafine nickel particles and polyanilines were studied by transmission electronmicroscopy (TEM), XRD, infraed spectrum (IR).
Key words:  Ultrafine nickel particle, Polyaniline, Inverse microemulsion systems, Nanocomposite particles
FundProject:
超微镍粒子/聚苯胺纳米复合材料制备及其表征
方鲲,李守平,崔陇兰,毛卫民,吴其晔*
摘要:
关键词:  超微镍粒子  聚苯胺  微乳液  纳米复合粒子
DOI:10.1088/1674-0068/16/3/163-165
分类号: