Fang Kun, Li Shouping, Cui Longlan, Mao Weimin, Wu Qiye. Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials[J]. Chinese Journal of Chemical Physics , 2003, 16(3): 163-165. doi: 10.1088/1674-0068/16/3/163-165
Citation: Fang Kun, Li Shouping, Cui Longlan, Mao Weimin, Wu Qiye. Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials[J]. Chinese Journal of Chemical Physics , 2003, 16(3): 163-165. doi: 10.1088/1674-0068/16/3/163-165

Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials

doi: 10.1088/1674-0068/16/3/163-165
  • Received Date: 2003-05-05
  • The ultrafine nickel particles/polyaniline nanocomposite materials were synthesized in situ polymerization by two step seriesW/O inverse microemulsion systems. As the first step, the ultrafine nickel nanoparticles whose diameter is 10~30 nm were prepared by the W/O inverse microemulsion systems and by the reduction. As the second step, the monomer aniline salt (AnH+Cl-) entered into the polar water pools where contained nickel nanoparticles and the ultrafine nickel particles/Polyaniline nanocomposite materials whose diameter is 50~100 nm had been obtained by in situ polymerization. These nanocomposite materials were measured to characterize and the micromorphology, microstructure and physical interaction of the both ultrafine nickel particles and polyanilines were studied by transmission electronmicroscopy (TEM), XRD, infraed spectrum (IR).
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials

doi: 10.1088/1674-0068/16/3/163-165

Abstract: The ultrafine nickel particles/polyaniline nanocomposite materials were synthesized in situ polymerization by two step seriesW/O inverse microemulsion systems. As the first step, the ultrafine nickel nanoparticles whose diameter is 10~30 nm were prepared by the W/O inverse microemulsion systems and by the reduction. As the second step, the monomer aniline salt (AnH+Cl-) entered into the polar water pools where contained nickel nanoparticles and the ultrafine nickel particles/Polyaniline nanocomposite materials whose diameter is 50~100 nm had been obtained by in situ polymerization. These nanocomposite materials were measured to characterize and the micromorphology, microstructure and physical interaction of the both ultrafine nickel particles and polyanilines were studied by transmission electronmicroscopy (TEM), XRD, infraed spectrum (IR).

Fang Kun, Li Shouping, Cui Longlan, Mao Weimin, Wu Qiye. Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials[J]. Chinese Journal of Chemical Physics , 2003, 16(3): 163-165. doi: 10.1088/1674-0068/16/3/163-165
Citation: Fang Kun, Li Shouping, Cui Longlan, Mao Weimin, Wu Qiye. Preparation and Characterization of Ultrafine Nickel Particles/Polyaniline Nanocomposite Materials[J]. Chinese Journal of Chemical Physics , 2003, 16(3): 163-165. doi: 10.1088/1674-0068/16/3/163-165

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