Song Xuchun, XuZhude, ChenWeixiang, ZhengYifan, HanGui. Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material[J]. Chinese Journal of Chemical Physics , 2004, 17(5): 629-632. doi: 10.1088/1674-0068/17/5/629-632
Citation: Song Xuchun, XuZhude, ChenWeixiang, ZhengYifan, HanGui. Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material[J]. Chinese Journal of Chemical Physics , 2004, 17(5): 629-632. doi: 10.1088/1674-0068/17/5/629-632

Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material

doi: 10.1088/1674-0068/17/5/629-632
Funds:  Project supported by the National Natural Science Foundation of China (20171039, 50171063).
  • Received Date: 2003-06-03
  • The Inorganic Fullerene-like MoS2 was obtained by a simple precipitation method using the polyethylenegly colas the dispersant,The hydroxylamine hydrochloride as the reductant, and (NH4)2S as the sulfursource. Themorphology and structure of the product were characterized by Powder X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and High-resolution Transmission Electron Microscopy (HRTEM). The results suggest that the polyethylene glycol dispersant can be adsorbed on the particle surface of the reaction precursor, amorphous MoS2 powders, to form a relative isolated environment. This isolated environment may induce an obstruct effect which helps the precursor nano-particles transfer to the IF structure in the subsequent calcinations process.
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material

doi: 10.1088/1674-0068/17/5/629-632
Funds:  Project supported by the National Natural Science Foundation of China (20171039, 50171063).

Abstract: The Inorganic Fullerene-like MoS2 was obtained by a simple precipitation method using the polyethylenegly colas the dispersant,The hydroxylamine hydrochloride as the reductant, and (NH4)2S as the sulfursource. Themorphology and structure of the product were characterized by Powder X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and High-resolution Transmission Electron Microscopy (HRTEM). The results suggest that the polyethylene glycol dispersant can be adsorbed on the particle surface of the reaction precursor, amorphous MoS2 powders, to form a relative isolated environment. This isolated environment may induce an obstruct effect which helps the precursor nano-particles transfer to the IF structure in the subsequent calcinations process.

Song Xuchun, XuZhude, ChenWeixiang, ZhengYifan, HanGui. Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material[J]. Chinese Journal of Chemical Physics , 2004, 17(5): 629-632. doi: 10.1088/1674-0068/17/5/629-632
Citation: Song Xuchun, XuZhude, ChenWeixiang, ZhengYifan, HanGui. Preparation and Characterization of Inorganic Fullerene-like MoS2 Nano-Material[J]. Chinese Journal of Chemical Physics , 2004, 17(5): 629-632. doi: 10.1088/1674-0068/17/5/629-632

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