Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO<sub>2</sub> Powder and Its Properties

Chen Zuyao; Qian Yitai; Zhao Yuwen; Li Yan; Wang Keqin; Fan Chenggao; Zhu Zhengang; Chen Zhaojia

Chen Zuyao, Qian Yitai, Zhao Yuwen, Li Yan, Wang Keqin, Fan Chenggao, Zhu Zhengang, Chen Zhaojia. Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO2 Powder and Its Properties[J]. Chinese Journal of Chemical Physics , 1991, 4(3): 227-230.

Citation:

Chen Zuyao, Qian Yitai, Zhao Yuwen, Li Yan, Wang Keqin, Fan Chenggao, Zhu Zhengang, Chen Zhaojia. Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO2 Powder and Its Properties[J]. Chinese Journal of Chemical Physics , 1991, 4(3): 227-230.

Citation:

Chen Zuyao, Qian Yitai, Zhao Yuwen, Li Yan, Wang Keqin, Fan Chenggao, Zhu Zhengang, Chen Zhaojia. Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO2 Powder and Its Properties[J]. Chinese Journal of Chemical Physics , 1991, 4(3): 227-230.

Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO₂ Powder and Its Properties

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Abstract

5nm ultrafine monoclinic ZrO₂ powder was prepared by hydrothermol method using zirconium nitrate solution in nitric acid. The particle size was determined by means of Electron Microscope and X-ray method. Measurement of specific heat was carried out and a abnormally higher specific heat at 90K to 160K was observed.

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Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO2 Powder and Its Properties

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Hydrothermol Preparation of 5-nm Nanocrystalline Monoclinic ZrO₂ Powder and Its Properties